E-ISSN 0976-2779 | ISSN 0975-8453
 

Review Article 


Study of the spectrophotometric determination of Nickel II ion by Michlerísthioketon Reagent

Husham Fathel Hashem, Alaa Frak Hussain.

Abstract
A new simple, rapid and sensitive spectrophotometric method has been develop to determine copper (–Ü) ions by using MichlerŘ•s thioketone reagent (Ligand) to formed a dark brown complex at ( pH=3) , The complex was found to be with stability for (90 min) at the given pH , The complex formed in this method give obeys Beerís law over the concentration range (3.211x10-5 MĖ22.48x10-5M) with a detection limit of (5.943x10-6 M) and molar absorptivity (5.122x103L.mol-1cm-1) ,The Stoichiometry of the complex was confirmed by using (Mole Ratio method and Molard method) the two methods using indicated the ratio of metal to reagent is 1:2,The effect of the presence of different cations and anions as interference in the determination of copper (–Ü) under the given condition were investigated, The copper complex formed has been characterize by UV- visible ray , Precision and accuracy of the new method has been study by terms of Relative standard deviations (RSD%), and relative error.

Key words: Michlerísthioketon, Reagent, Stoichometry, absorptivity


 
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Pubmed Style

Husham Fathel Hashem, Alaa Frak Hussain. Study of the spectrophotometric determination of Nickel II ion by Michlerísthioketon Reagent. SRP. 2021; 12(2): 336-341. doi:10.31838/srp.2021.2.45


Web Style

Husham Fathel Hashem, Alaa Frak Hussain. Study of the spectrophotometric determination of Nickel II ion by Michlerísthioketon Reagent. http://www.sysrevpharm.org/?mno=35022 [Access: January 22, 2021]. doi:10.31838/srp.2021.2.45


AMA (American Medical Association) Style

Husham Fathel Hashem, Alaa Frak Hussain. Study of the spectrophotometric determination of Nickel II ion by Michlerísthioketon Reagent. SRP. 2021; 12(2): 336-341. doi:10.31838/srp.2021.2.45



Vancouver/ICMJE Style

Husham Fathel Hashem, Alaa Frak Hussain. Study of the spectrophotometric determination of Nickel II ion by Michlerísthioketon Reagent. SRP. (2021), [cited January 22, 2021]; 12(2): 336-341. doi:10.31838/srp.2021.2.45



Harvard Style

Husham Fathel Hashem, Alaa Frak Hussain (2021) Study of the spectrophotometric determination of Nickel II ion by Michlerísthioketon Reagent. SRP, 12 (2), 336-341. doi:10.31838/srp.2021.2.45



Turabian Style

Husham Fathel Hashem, Alaa Frak Hussain. 2021. Study of the spectrophotometric determination of Nickel II ion by Michlerísthioketon Reagent. Systematic Reviews in Pharmacy, 12 (2), 336-341. doi:10.31838/srp.2021.2.45



Chicago Style

Husham Fathel Hashem, Alaa Frak Hussain. "Study of the spectrophotometric determination of Nickel II ion by Michlerísthioketon Reagent." Systematic Reviews in Pharmacy 12 (2021), 336-341. doi:10.31838/srp.2021.2.45



MLA (The Modern Language Association) Style

Husham Fathel Hashem, Alaa Frak Hussain. "Study of the spectrophotometric determination of Nickel II ion by Michlerísthioketon Reagent." Systematic Reviews in Pharmacy 12.2 (2021), 336-341. Print. doi:10.31838/srp.2021.2.45



APA (American Psychological Association) Style

Husham Fathel Hashem, Alaa Frak Hussain (2021) Study of the spectrophotometric determination of Nickel II ion by Michlerísthioketon Reagent. Systematic Reviews in Pharmacy, 12 (2), 336-341. doi:10.31838/srp.2021.2.45





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