Synthesis And Characterization Of Fluorescent Schiff Bases And Their Metal Complexes From 9- Anthracenecarboxaldehy
Abstract
Inam hassim ibrahim, Hasan A. Hasan.
Synthesis and characterisation two Schiff bases[L1] (N2Z,N6Z)-N2,N6-bis(4-((E)- anthracen-9-ylmethyleneamino)-1,5-dimethyl-2- phenyl-1H-pyrazol-3(2H)- ylidene)pyridine-2,6-diamine Synthesis via reaction of 2,6-diaminopyridine, 4- aminoantipyrine and 9- anthracenecarboxaldehyde with mole ratio (1:2:2) respectively two steps. And[L2] (N1Z,N2Z)-N1,N2-bis(4-((E)-anthracen-9- ylmethyleneamino)- 1,5-dimethyl-2- phenyl-1H-pyrazol-3(2H)-ylidene)-4- methylbenzene-1,2-diamine Synthesis from reaction of o-phenylendiamine ,4- aminoantipyrine and 9-anthracenecarboxaldehyde with mole ratio (1:2:2) respectively two steps. A new series of transition metal complexes of Mn(II), Co(II), Ca(II), Cd(II) , Zn(II) and pd(II) were synthesized .The structural features were derived from their elemental analyses, infrared, UV-visible spectroscopy, 1HNMR,13CNMR spectroscopy, thermal gravimetric analyses spectral ,magnetic susceptibility measurement, chloride content and conductivity measurements. The electronic spectral data and magnetic measurements indicate that the complexes exhibit octahedral geometry around Ca(II), Mn(II), Cd(II), Co(II), Zn(II) while Square planer geometry around Pd(II).
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| Pubmed Style Inam hassim ibrahim, Hasan A. Hasan. Synthesis And Characterization Of Fluorescent Schiff Bases And Their Metal Complexes From 9- Anthracenecarboxaldehy. SRP. 2021; 12(1): 306-314. doi:10.31838/srp.2021.1.41 Web Style Inam hassim ibrahim, Hasan A. Hasan. Synthesis And Characterization Of Fluorescent Schiff Bases And Their Metal Complexes From 9- Anthracenecarboxaldehy. http://www.sysrevpharm.org/?mno=32902 [Access: March 29, 2021]. doi:10.31838/srp.2021.1.41 AMA (American Medical Association) Style Inam hassim ibrahim, Hasan A. Hasan. Synthesis And Characterization Of Fluorescent Schiff Bases And Their Metal Complexes From 9- Anthracenecarboxaldehy. SRP. 2021; 12(1): 306-314. doi:10.31838/srp.2021.1.41 Vancouver/ICMJE Style Inam hassim ibrahim, Hasan A. Hasan. Synthesis And Characterization Of Fluorescent Schiff Bases And Their Metal Complexes From 9- Anthracenecarboxaldehy. SRP. (2021), [cited March 29, 2021]; 12(1): 306-314. doi:10.31838/srp.2021.1.41 Harvard Style Inam hassim ibrahim, Hasan A. Hasan (2021) Synthesis And Characterization Of Fluorescent Schiff Bases And Their Metal Complexes From 9- Anthracenecarboxaldehy. SRP, 12 (1), 306-314. doi:10.31838/srp.2021.1.41 Turabian Style Inam hassim ibrahim, Hasan A. Hasan. 2021. Synthesis And Characterization Of Fluorescent Schiff Bases And Their Metal Complexes From 9- Anthracenecarboxaldehy. Systematic Reviews in Pharmacy, 12 (1), 306-314. doi:10.31838/srp.2021.1.41 Chicago Style Inam hassim ibrahim, Hasan A. Hasan. "Synthesis And Characterization Of Fluorescent Schiff Bases And Their Metal Complexes From 9- Anthracenecarboxaldehy." Systematic Reviews in Pharmacy 12 (2021), 306-314. doi:10.31838/srp.2021.1.41 MLA (The Modern Language Association) Style Inam hassim ibrahim, Hasan A. Hasan. "Synthesis And Characterization Of Fluorescent Schiff Bases And Their Metal Complexes From 9- Anthracenecarboxaldehy." Systematic Reviews in Pharmacy 12.1 (2021), 306-314. Print. doi:10.31838/srp.2021.1.41 APA (American Psychological Association) Style Inam hassim ibrahim, Hasan A. Hasan (2021) Synthesis And Characterization Of Fluorescent Schiff Bases And Their Metal Complexes From 9- Anthracenecarboxaldehy. Systematic Reviews in Pharmacy, 12 (1), 306-314. doi:10.31838/srp.2021.1.41 |
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